Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl chloride → 3-Benzoyloxy-5-methylisoxazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl chloride | HCID 7412 | — |
| 반응물 | Hymexazol | HCID 24781 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 3-Benzoyloxy-5-methylisoxazole | HCID 12415007 | — |
반응 단계
3-Hydroxy-5-methylisoxazole was reacted with benzoyl chloride in the presence of triethylamine to give 3-benzoyloxy-5-methylisoxazole, which was then reacted with N-bromosuccinimide, to give 3-benzoyloxy-5-bromomethylisoxazole. This was reacted with disodium thioglycolate to give 3-hydroxyisoxazol-5-ylmethylthioacetic acid, which was treated with diphenyldiazomethane to give the benzhydryl ester.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04247548 |
| 출처 데이터셋 | uspto-grants-1981_01 |
| ORD ID | ord-784b205c021847b0b97909951156c164 |
| 출처 메모 | uspto-grants-1981_01 |