Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4,4-Bis(methoxymethyl)biphenyl → [1,1'-Biphenyl]-4,4'-dicarboxaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4,4-Bis(methoxymethyl)biphenyl | HCID 1519430 | — |
| 반응물 | Sodium Bromate | HCID 23668195 | — |
| 생성물 | [1,1'-Biphenyl]-4,4'-dicarboxaldehyde | HCID 6200 | — |
반응 단계
In the same manner as in Example 3, the operation was conducted, except that 0.53 g (2 mmols) of bismethoxymethylbiphenyl was used in place of m-methoxybenzyl alcohol and also 0.2 g (1.35 mmols) of sodium bromate was used. With respect to the components in the reaction solution, 4,4′-bisformylbiphenyl was produced in an area ratio, as determined by gas chromatography, of 93.3% and 6.7% of bismethoxymethylbiphenyl as a raw material was remained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07342138B2 |
| 출처 데이터셋 | uspto-grants-2008_03 |
| ORD ID | ord-5860edf70f8347c2b5e0d67f6c44c247 |
| 출처 메모 | uspto-grants-2008_03 |