Aluminium lithium hydride → HCID 15676492, 화합물

HRID 1393353노트

반응식

HRID 1393353 반응식
[C:1]1([C:7]2[S:8][C:9]3[C:15]([C:16](O)=[O:17])=[CH:14][CH:13]=[CH:12][C:10]=3[N:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[C:1]1([C:7]2[S:8][C:9]3[C:15]([CH2:16][OH:17])=[CH:14][CH:13]=[CH:12][C:10]=3[N:11]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

3

반응물 2

HCID 21226445Aluminium lithium hydrideHCID 23033929HCID 23033929, 화합물

생성물 1

HCID 15676492HCID 15676492, 화합물수율 94%

실험 절차

Ethyl ester of 2-phenylbenzothiazole-7-carboxylic acid (425 mg, 1.50 mmol) was reduced by using lithium aluminium hydride as in Preparation 2-3) to give 2-phenylbenzothiazole-7-methanol (340 mg, 94%) as colorless crystals.

후처리

  1. customas in Preparation 2-3)

출처 및 근거

ORD 기록
ord-d41e14f3a4ec45a7a37f92f34bb13dba
출처 데이터셋
uspto-grants-2008_03
특허 번호
US07345068B2

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