참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3,5-Dimethylaniline | HCID 7949 | — |
| 반응물 | 3-Fluoro-4-nitrophenol | HCID 520948 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 3-(3,5-Dimethylphenyl)amino-4-nitrophenol | HCID 21938154 | — |
반응 단계
5.4 g of 3-fluoro-4-nitrophenol and 4.3 ml of 3,5-dimethylaniline were mixed and stirred for 6 hours at 120° C. After cooling, it was taken up in ethyl acetate and water and extracted three times with 1N aqueous hydrochloric acid. The combined aqueous phases were extracted three times with ethyl acetate. The combined organic phases were dried on sodium sulfate, concentrated by evaporation in a vacuum, and the residue was crystallized.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07345075B2 |
|---|
| 출처 데이터셋 | uspto-grants-2008_03 |
|---|
| ORD ID | ord-bcea5b27711246bcb25a415921eaedd6 |
|---|
| 출처 메모 | uspto-grants-2008_03 |
|---|
