HCID 178458089, 화합물 → HCID 178458088, 화합물

HRID 1393922노트

반응식

HRID 1393922 반응식
C(OC([NH:11][C@:12]1([PH:20]([NH:22][CH2:23][CH2:24][CH3:25])=[O:21])[CH2:17][CH2:16][CH2:15][N:14]([NH2:18])[C:13]1=[O:19])=O)C1C=CC=CC=1>CO.[Pd]>[NH2:11][C:12]1([PH:20]([NH:22][CH2:23][CH2:24][CH3:25])=[O:21])[CH2:17][CH2:16][CH2:15][N:14]([NH2:18])[C:13]1=[O:19]

참가 물질

4

반응물 1

HCID 178458089HCID 178458089, 화합물

생성물 1

HCID 178458088HCID 178458088, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

Palladium black (16 mg) was added to a solution of (3S)-3-benzyloxycarbonylamino-1-amino(n-propylamino)phosphinyl-2-piperidone (161.1 g, 0.4373 mmol) in methanol (3 mL), and the resulting mixture was stirred at room temperature for 50 minutes under a hydrogen atmosphere.

출처 및 근거

ORD 기록
ord-c44e1675fede41c9991429b04438c544
출처 데이터셋
uspto-grants-2008_03
특허 번호
US07348318B2

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