Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromopropane → Isopropyl(2-nitrophenyl)sulfane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromopropane | HCID 6358 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | o-Nitrobenzenethiol | HCID 21002 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | Isopropyl(2-nitrophenyl)sulfane | HCID 12505026 | — |
반응 단계
2-Nitrothiophenol, 2-bromopropane, potassium carbonate and acetone were refluxed for several hours. The solvent then was removed by rotary evaporation. The crude product was partitioned between methylene chloride and a 10% sodium carbonate solution. The organic phase was distilled to yield 2-isopropylmercaptonitrobenzene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04202821 |
| 출처 데이터셋 | uspto-grants-1980_05 |
| ORD ID | ord-d6d6d8edf9324ff78a7de0fc55818bb5 |
| 출처 메모 | uspto-grants-1980_05 |