Thionyl Chloride → HCID 20338242, 화합물

HRID 1395805노트

반응식

HRID 1395805 반응식
[CH2:1]([N:8]([CH2:18][CH2:19]O)[C:9]1[CH:17]=[CH:16][CH:15]=[CH:14][C:10]=1[C:11]([NH2:13])=[O:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.O=S(Cl)[Cl:23]>>[ClH:23].[CH2:1]([N:8]([CH2:18][CH2:19][Cl:23])[C:9]1[CH:17]=[CH:16][CH:15]=[CH:14][C:10]=1[C:11]([NH2:13])=[O:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 24386Thionyl ChlorideHCID 203383632-[Benzyl(2-hydroxyethyl)amino]benzamide

생성물 1

HCID 20338242HCID 20338242, 화합물

실험 절차

2-[Benzyl(2-hydroxyethyl)amino]benzamide (10 g) was added at 0° to 50 ml SOCl2, stirred 71/2 hours at room temperature and left overnight. The mixture was concentrated on the rotovap, ethyl acetate added and the solid filtered to give 11 g product, m.171-4.

후처리

  1. waitleft overnight
  2. concentrationThe mixture was concentrated on the rotovap, ethyl acetate
  3. additionadded
  4. filtrationthe solid filtered

출처 및 근거

ORD 기록
ord-9894977ada49490693913a6fc704a3ad
출처 데이터셋
uspto-grants-1980_05
특허 번호
US04205173

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