2-Thiophenecarboxaldehyde, 5-chloro- → HCID 59053600, 화합물

반응식

[Cl-].[F:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][C:4]=1[O:13][CH2:14][CH2:15][NH3+:16].[Cl:17][C:18]1[S:22][C:21]([CH:23]=O)=[CH:20][CH:19]=1>>[Cl:17][C:18]1[S:22][C:21]([CH2:23][NH:16][CH2:15][CH2:14][O:13][C:4]2[CH:5]=[CH:6][C:7]3[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=3)[C:3]=2[F:2])=[CH:20][CH:19]=1

참가 물질

반응물 2

HCID 817002-Thiophenecarboxaldehyde, 5-chloro-

HCID 68151396HCID 68151396, 화합물

생성물 1

HCID 59053600HCID 59053600, 화합물수율 71%

실험 절차

Prepared from 2-[(1-fluoronaphthalen-2-yl)oxy]ethanaminium chloride and 5-chlorothiophen-2-carbaldehyde in 71% yield as a slightly white oil.

출처 및 근거

ORD 기록: ord-ca0d4e8d050e49bba39363f68f72c477
출처 데이터셋: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08906946B2

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