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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1401188생성일: 2026년 10월 27일

1,1-Bis(2,2-dimethylpropoxy)-N,N-dimethylmethanamine → HCID 178496568, 화합물

https://huagongshe.com/reaction/1401188

반응식

참여 물질

역할이름HCID투입량
반응물1,1-Bis(2,2-dimethylpropoxy)-N,N-dimethylmethanamineHCID 78623—
반응물HCID 178496567HCID 178496567—
용매TetrahydrofuranHCID 8028—
생성물HCID 178496568HCID 178496568100%

반응 조건

온도85 °C

반응 단계

5-(8-(((trans)-4-Methoxycyclohexyl)methyl)-7-oxo-5,6,7,8-tetrahydropyrazino[2,3-b]pyrazin-2-yl)-4-methylpicolinamide (0.412 g, 1.00 mmol), dimethylformamide dineopentylacetal (1.5 mL) and tetrahydrofuran (10 mL) were combined and heated at 85° C. for 3 h. Reaction was concentrated under a stream of nitrogen placed in reaction vessel. Crude product was used directly for next step (0.467 g, 1.00 mmol, 100% yield). MS (ESI) m/z 466.6 [M+1]+

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08907087B2
출처 데이터셋uspto-grants-2014_12
ORD IDord-6a4d283a37ec4956b9c8ff36ed9b27b1
출처 메모uspto-grants-2014_12