2-Acetylnaphthalene → HCID 3965467, 화합물

HRID 1402967노트

반응식

HRID 1402967 반응식
[C:1]1([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:6]=[CH:5][C:4]([CH:7]=O)=[CH:3][CH:2]=1.[CH:15]1[C:24]2[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=2)[CH:18]=[CH:17][C:16]=1[C:25](=[O:27])[CH3:26]>>[C:1]1([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:6]=[CH:5][C:4]([CH:7]=[CH:26][C:25]([C:16]2[CH:17]=[CH:18][C:19]3[C:24](=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH:15]=2)=[O:27])=[CH:3][CH:2]=1

참가 물질

3

반응물 2

HCID 71222-AcetylnaphthaleneHCID 76689(1,1'-Biphenyl)-4-carboxaldehyde

생성물 1

HCID 3965467HCID 3965467, 화합물

실험 절차

Synthesised according to example 1.59.1 using biphenyl-4-carbaldehyde (5.0 g, 29.3 mmol) and 1-(naphthalen-2-yl)ethanone (5.35 g, 29.3 mmol); yellow solid; yield: 7.80 g (79%);

후처리

  1. customSynthesised

출처 및 근거

ORD 기록
ord-f52833ba999c4890a5c0f12be432745a
출처 데이터셋
uspto-grants-2014_12
특허 번호
US08912186B2

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