3-Methylbenzyl alcohol → HCID 66576055, 화합물

HRID 1405252

반응식

HRID 1405252 반응식
F[C:2]1[CH:7]=[C:6]([F:8])[CH:5]=[CH:4][C:3]=1[C:9]1[N:14]=[CH:13][N:12]=[C:11]([NH:15][C:16]2[CH:21]=[CH:20][CH:19]=[C:18]([CH2:22][S:23]([CH3:26])(=[O:25])=[O:24])[CH:17]=2)[N:10]=1.[CH3:27][C:28]1[CH:29]=[C:30]([CH:33]=[CH:34][CH:35]=1)[CH2:31][OH:32]>>[F:8][C:6]1[CH:5]=[CH:4][C:3]([C:9]2[N:14]=[CH:13][N:12]=[C:11]([NH:15][C:16]3[CH:21]=[CH:20][CH:19]=[C:18]([CH2:22][S:23]([CH3:26])(=[O:25])=[O:24])[CH:17]=3)[N:10]=2)=[C:2]([O:32][CH2:31][C:30]2[CH:33]=[CH:34][CH:35]=[C:28]([CH3:27])[CH:29]=2)[CH:7]=1

참가 물질

3

반응물 2

HCID 114763-Methylbenzyl alcoholHCID 709765244-(2,4-difluorophenyl)-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine

생성물 1

HCID 66576055HCID 66576055, 화합물

실험 절차

Starting with 4-(2,4-difluorophenyl)-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine (75 mg; 0.197 mmol), intermediate 42.1, and 3-methylbenzyl alcohol (99 mg; 0.789 mmol), example 83 was prepared analogously to the procedure for the preparation of example 42.

후처리

  1. customwas prepared analogously to the procedure for the preparation of example 42

출처 및 근거

ORD 기록
ord-82baf5fabdf84d64848de86e40bc170e
출처 데이터셋
uspto-grants-2014_12
특허 번호
US08916557B2

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