Methanol → HCID 53663529, 화합물
반응식
C([O:8][C:9]([NH:11][CH2:12][CH2:13][S:14]([NH2:17])(=[O:16])=[O:15])=O)C1C=CC=CC=1.CO>[Pd].C(O)=O>[CH:9]([NH:11][CH2:12][CH2:13][S:14]([NH2:17])(=[O:16])=[O:15])=[O:8]참가 물질
5
실험 절차
In a reaction flask, 10.3 g of 2-benzyloxyformamidoethylsulfonamide, 10% Pd/C (3.0 g) and 600 ml of methanol were added. The mixture was stirred at room temperature overnight under hydrogen atmosphere, added with 35 ml of formic acid, stirred for 30 min, filtered, and concentrated under a reduced pressure to obtain 5.6 g of oily product, yield 93%.
후처리
- stirringstirred for 30 min
- filtrationfiltered
- concentrationconcentrated under a reduced pressure
출처 및 근거
- ORD 기록
- ord-295e840ebcbc4de99c2ded232ca6a24d
- 출처 데이터셋
- uspto-grants-2014_12
- 특허 번호
- US08916574B2
반응 노트
불러오는 중…