Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3,2-Dioxathiolane, 2,2-dioxide → Cyclohexylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3,2-Dioxathiolane, 2,2-dioxide | HCID 14075 | — |
| 반응물 | 3,3-Diphenylpropyl methyl ammonium chloride | HCID 21467371 | — |
| 반응물 | Butyllithium | HCID 178418339 | — |
| 생성물 | Cyclohexylamine | HCID 7965 | — |
| 생성물 | n-Hexyl sulphate lithium salt | HCID 23693704 | — |
반응 단계
N-methyl-3,3-diphenyl-propylamine hydrochloride, m.p. 159°-61° C. By a procedure analogous to that given above ethylene sulphate is reacted with butyllithium to give n-hexyl sulphate lithium salt which with cyclohexylamine gives N-cyclohexyl-n-hexylamine (b.p. 66° C./0.6).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04249003 |
| 출처 데이터셋 | uspto-grants-1981_02 |
| ORD ID | ord-3aaa0806a3534c77a7e2bc244df9db2b |
| 출처 메모 | uspto-grants-1981_02 |