Diphenyl Ether → HCID 13548752, 화합물

반응식

C[S:2][C:3](=S)[NH:4][N:5]=[CH:6][C:7]1[N:8]=[C:9]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[NH:10][C:11]=1[CH3:12].C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH3:12][C:11]1[N:10]=[C:9]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[N:8]2[C:7]=1[CH:6]=[N:5][NH:4][C:3]2=[S:2]

참가 물질

반응물 2

HCID 7583Diphenyl Ether

HCID 136020036HCID 136020036, 화합물

생성물 1

HCID 13548752HCID 13548752, 화합물

실험 절차

A mixture of 73.4 gm. of 3-[(5-methyl-2-phenyl-4-imidazolyl)methylene]dithiocarbazic acid methyl ester and 500 ml. of diphenyl ether is reacted as described in Example 58 giving the desired product as purple crystals, m.p. 237.5°-239° C.

후처리

additionA mixture of 73.4 gm

출처 및 근거

ORD 기록: ord-78bdc0e2c9474caaad6a962e82fbdf93
출처 데이터셋: uspto-grants-1981_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: USRE030511

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