Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Butyric acid, 4-(p-chloro-N-2,6-xylylbenzamido)- → methyl N-[N-(p-chlorobenzoyl)-4-(2,6dimethylanilino)butyryl]-L-alaninate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Butyric acid, 4-(p-chloro-N-2,6-xylylbenzamido)- | HCID 35383 | — |
| 반응물 | L-Alanine methyl ester | HCID 82335 | — |
| 생성물 | methyl N-[N-(p-chlorobenzoyl)-4-(2,6dimethylanilino)butyryl]-L-alaninate | HCID 22814603 | — |
반응 단계
Analogously to Example 1, by using equivalent quantities, reacting N-(p-chlorobenzoyl)-4-(2,6-dimethylanilino)butyric acid and methyl L-alaninate and suitable processing produces methyl N-[N-(p-chlorobenzoyl)-4-(2,6dimethylanilino)butyryl]-L-alaninate (M.P. 91° to 92°), saponification of which and processing of the reaction product yields N-[N-(p-chlorobenzoyl)-4-(2,6-dimethylanilino)butyryl]-L-alanine (M.P. 159° to 161°).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04250183 |
| 출처 데이터셋 | uspto-grants-1981_02 |
| ORD ID | ord-ee1dc04540464853bfcc9edf947574eb |
| 출처 메모 | uspto-grants-1981_02 |