Fumarate → 3',4'-Dichloro-2-(2-pyrrolidinylidene)-acetophenone
반응식
[Cl:1][C:2]1[CH:3]=[C:4]([C:9](=NC2CCCCC2)[CH:10]=[C:11]2[CH2:15][CH2:14][CH2:13][NH:12]2)[CH:5]=[CH:6][C:7]=1[Cl:8].C([O-])(=O)/C=C/C([O-])=[O:27]>C(O)(C)C.CCOCC>[Cl:1][C:2]1[CH:3]=[C:4]([C:9](=[O:27])[CH:10]=[C:11]2[CH2:15][CH2:14][CH2:13][NH:12]2)[CH:5]=[CH:6][C:7]=1[Cl:8]참가 물질
4
실험 절차
With the use of 76.8 g (0.3 mole) of 3',4'-dichloro-2-(2-pyrrolidinylidene)-acetophenone, there is obtained in an analogous manner 2-[2-(3,4-dichlorophenyl)-2-(cyclohexylimino)-ethylidene]-pyrrolidine-(1:1)-fumarate, m.p. 208°-209° (from isopropanol/ether).
출처 및 근거
- ORD 기록
- ord-1a70ff95076948fbbb885b302a7f4799
- 출처 데이터셋
- uspto-grants-1981_02
- 특허 번호
- US04251542
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