Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methyl-1-phenylthiourea → 3-Methyl-1,3-benzothiazol-2(3H)-imine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methyl-1-phenylthiourea | HCID 723631 | — |
| 반응물 | Thiourea, N-ethyl-N-phenyl- | HCID 825369 | — |
| 생성물 | 3-Methyl-1,3-benzothiazol-2(3H)-imine | HCID 84642 | 95.6% |
반응 단계
When the reaction is carried out as described in Example 23 with the exception that instead of N-ethyl-N-phenylthiourea an equimolar amount of N-methyl-N-phenylthiourea is used, 3-methyl-2-iminobenzthiazoline melting at 122° C. is obtained in a yield of 95.6% and with an equally good purity.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04252963 |
| 출처 데이터셋 | uspto-grants-1981_02 |
| ORD ID | ord-02268f29120d4621a346bb76db2ca2a2 |
| 출처 메모 | uspto-grants-1981_02 |