Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
9,10-Anthracenedione, 2-amino-3-chloro- → Anthrimide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 9,10-Anthracenedione, 2-amino-3-chloro- | HCID 6771 | — |
| 반응물 | Nitrobenzene | HCID 7416 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 1-Amino-4-chloro-9,10-anthracenedione | HCID 17884 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | Anthrimide | HCID 6700 | — |
반응 단계
21 g of 6-chloro-2-(4-diphenyl)-anthrapyrimidine (obtained by reacting 1-amino-4-chloroanthraquinone with diphenyl-4-carboxylic acid N-methylamide in the presence of thionyl chloride (in accordance with D.R.P. 566,474)) are condensed, in accordance with Example 1, in 250 parts of nitrobenzene in the presence of 7.5 parts of sodium carbonate and 0.25 part of copper-1 chloride with 13.5 parts of 1-amino-3-chloroanthraquinone. 28 parts are obtained of the anthrimide of the formula ##SPC9##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04001170 |
| 출처 데이터셋 | uspto-grants-1977_01 |
| ORD ID | ord-9382bbe1a6aa4dd395b41c896390f9e5 |
| 출처 메모 | uspto-grants-1977_01 |