3,5-Dimethylbenzoyl Chloride → HCID 21487907, 화합물

반응식

[Cl:1][CH2:2][CH2:3][O:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]2[O:12][C:13]3[CH:19]=[CH:18][C:17]([O:20][CH3:21])=[CH:16][C:14]=3[CH:15]=2)=[CH:7][CH:6]=1.[CH3:22][C:23]1[CH:24]=[C:25]([CH:29]=[C:30]([CH3:32])[CH:31]=1)[C:26](Cl)=[O:27]>>[Cl:1][CH2:2][CH2:3][O:4][C:5]1[CH:6]=[CH:7][C:8]([C:11]2[O:12][C:13]3[CH:19]=[CH:18][C:17]([O:20][CH3:21])=[CH:16][C:14]=3[C:15]=2[C:26](=[O:27])[C:25]2[CH:29]=[C:30]([CH3:32])[CH:31]=[C:23]([CH3:22])[CH:24]=2)=[CH:9][CH:10]=1

참가 물질

반응물 2

HCID 810883,5-Dimethylbenzoyl Chloride

HCID 21487986HCID 21487986, 화합물

생성물 1

HCID 21487907HCID 21487907, 화합물

실험 절차

Acylation of 2-[4'-(2-chloroethoxy)phenyl]-5-methoxybenzofuran with 3,5-dimethylbenzoyl chloride as described in the procedure of Example 11 gives 2-[4'-(2-chloroethoxy)phenyl]-5-methoxy-3-(3',5'-dimethylbenzoyl)benzofuran.

출처 및 근거

ORD 기록: ord-e74fd8e2a8764074bfdcd07895f807a9
출처 데이터셋: uspto-grants-1977_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04001426

반응 노트

불러오는 중…