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2-Amino-3-hydroxyoctanoic acid → HCID 21416538, 화합물

HRID 1414702
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HRID 1414702 반응식
NC(C(O)CCCCC)C(O)=O.[C:13]([NH:16][CH:17]([CH:21]([OH:27])[CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[C:18](O)=[O:19])(=[O:15])[CH3:14].COC(=O)C(NC(=O)C)C(O)CCCCC.[H-].C([Al+]CC(C)C)C(C)C>CO>[C:13]([NH:16][CH:17]([CH:21]([OH:27])[CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[CH:18]=[O:19])(=[O:15])[CH3:14]
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6

반응물 4

HCID 187908012-Amino-3-hydroxyoctanoic acidHCID 21225700DiisobutylaluminumhydrideHCID 21416541HCID 21416541, 화합물HCID 53991059HCID 53991059, 화합물

생성물 1

HCID 21416538HCID 21416538, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Protect the amino function in the 2-amino-3-hydroxyoctanoic acid by conversion thereof to an acetamido function, then esterify the resultant 2-acetamido-3-hydroxyoctanoic acid with methanol; reduce the resultant 2-acetamido-3-hydroxyoctanoic acid methyl ester with di-isobutylaluminum hydride according to known procedures to obtain 2-acetamido-3-hydroxyoctanal.

출처 및 근거

ORD 기록
ord-80bcba4fcc5940688da9bf420cede3fb
출처 데이터셋
uspto-grants-1977_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04002608

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