반응식
[Cl:1][C:2]1[C:3]([CH2:8][CH2:9][CH2:10][CH2:11][NH2:12])=[N:4][CH:5]=[CH:6][CH:7]=1.[C:13]([CH:15]=[C:16](OCC)[NH:17][CH3:18])#[N:14]>>[C:13]([CH:15]=[C:16]([NH:17][CH3:18])[NH:12][CH2:11][CH2:10][CH2:9][CH2:8][C:3]1[C:2]([Cl:1])=[CH:7][CH:6]=[CH:5][N:4]=1)#[N:14]참가 물질
3
실험 절차
3-Chloro-2-(4-aminobutyl)pyridine is added to a solution of 1-cyano-2-ethoxy-2-methylaminoethylene and stirred at 100° for 5 hours. Chromatographic purification of the reaction mixture yields the title compound.
후처리
- customChromatographic purification of the reaction mixture
출처 및 근거
- ORD 기록
- ord-6bcc114d361a4e798951c384bf65da2d
- 출처 데이터셋
- uspto-grants-1977_01
- 특허 번호
- US04002759
연결된 노트
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