Trimethylamine → HCID 70632541, 화합물

HRID 1415444노트

반응식

HRID 1415444 반응식
Br[CH2:2][Si:3]([CH3:8])([O:6][CH3:7])[O:4][CH3:5].CN[CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.[CH3:18][N:19](C)C>CCCCCC>[CH2:11]([CH2:18][NH:19][CH2:2][Si:3]([CH3:8])([O:6][CH3:7])[O:4][CH3:5])[C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1

참가 물질

5

반응물 3

HCID 1146TrimethylamineHCID 7669N-MethylbenzylamineHCID 21481846HCID 21481846, 화합물

생성물 1

HCID 70632541HCID 70632541, 화합물

시약·촉매·용매 1

HCID 8058Hexane용매

반응 조건

온도
100 °C

실험 절차

To 0.25 moles of bromomethylmethyldimethoxysilane is added 0.25 moles of methylbenzylamine, and the mixture is heated to 100° C. for 12 hours. At the end of that time, 300 ml of hexane is added and excess trimethylamine is added. This mixture is allowed to stir for 3 hours, filtered, and the hexane is removed under reduced pressure, leaving benzylmethylaminomethylmethyldimethoxysilane.

후처리

  1. filtrationfiltered
  2. customthe hexane is removed under reduced pressure

출처 및 근거

ORD 기록
ord-521d2d6b9e16418fa22849a04c213d75
출처 데이터셋
uspto-grants-1977_01
특허 번호
US04005118

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