Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Di(tetrachlorophenyl)tetrachlorocyclopentadiene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Hexachlorocyclopentadiene | HCID 6478 | — |
| 반응물 | 1,2,3,4-Tetrachlorobenzene | HCID 12463 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 생성물 | Di(tetrachlorophenyl)tetrachlorocyclopentadiene | HCID 54039303 | — |
반응 단계
A mixture of 1,2,3,4-tetrachlorobenzene, 130 grams (0.6 mole), hexachlorocyclopentadiene, 65 grams (0.24 mole), and aluminum chloride, 5 grams, was heated on a steam bath at 75°-90° centigrade until the evolution of hydrogen chloride stopped and the reaction mixture solidified. The purple solid was triturated with acetone to dissolve the aluminum chloride, filtered, washed with acetone and dried to give a tan, solid product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04005153 |
| 출처 데이터셋 | uspto-grants-1977_01 |
| ORD ID | ord-b9208cc0342340e587b3093fb7374cf0 |
| 출처 메모 | uspto-grants-1977_01 |