Isopropylamine → HCID 21482733, 화합물

HRID 1415505노트

반응식

HRID 1415505 반응식
[Br:1][C:2]1[CH:3]=[C:4]([S:9](Cl)(=[O:11])=[O:10])[CH:5]=[C:6]([Br:8])[CH:7]=1.[CH:13]([NH2:16])([CH3:15])[CH3:14]>O>[Br:1][C:2]1[CH:3]=[C:4]([S:9]([NH:16][CH:13]([CH3:15])[CH3:14])(=[O:11])=[O:10])[CH:5]=[C:6]([Br:8])[CH:7]=1

참가 물질

4

반응물 2

HCID 6363IsopropylamineHCID 214827463,5-Dibromobenzene-1-sulfonyl chloride

생성물 1

HCID 21482733HCID 21482733, 화합물

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

3.0 G. of 3,5-dibromobenzenesulfonylchloride is added to a solution of 17.7 g. of isopropylamine in 25 ml. of water at room temperature. A complete solution results which is stirred for 2 hours and poured onto 250 ml. of water. The precipitate is filtered, washed with water, and dried affording 3,5-dibromo-N-isopropylbenzenesulfonamide, m.p. 105° to 107° C.

후처리

  1. customat room temperature
  2. customA complete solution results which
  3. additionpoured onto 250 ml
  4. filtrationThe precipitate is filtered
  5. washwashed with water
  6. customdried

출처 및 근거

ORD 기록
ord-93082192e85242618a8ecc23c1eaa4d3
출처 데이터셋
uspto-grants-1977_01
특허 번호
US04005199

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