1-Propanol → n-Propyl ferulate

HRID 1415660

반응식

HRID 1415660 반응식
[C:1]([OH:14])(=[O:13])/[CH:2]=[CH:3]/[C:4]1[CH:12]=[CH:11][C:9]([OH:10])=[C:6]([O:7][CH3:8])[CH:5]=1.[CH2:15](O)[CH2:16][CH3:17]>C1C=CC=CC=1>[C:1]([O:14][CH2:15][CH2:16][CH3:17])(=[O:13])/[CH:2]=[CH:3]/[C:4]1[CH:12]=[CH:11][C:9]([OH:10])=[C:6]([O:7][CH3:8])[CH:5]=1

참가 물질

4

반응물 2

HCID 10311-PropanolHCID 445858Ferulic Acid

생성물 1

HCID 9881169n-Propyl ferulate수율 64.3%

시약·촉매·용매 1

HCID 241Benzene용매

반응 조건

온도
78 °C

실험 절차

In a three-necked flask, 19.4 g (0.1 mole) of ferulic acid, 6.01 g (0.1 mole) of n-propyl alcohol, and 1.0 g of paratoluenesulfonic acid were placed, and 200 ml of benzene was added. This reaction mixture was stirred at 78° C. for 15 hours. Thereafter, the same procedures were taken as in Example 1 to obtain 15.2 g (yield: 64%) of n-propyl ferulate.

출처 및 근거

ORD 기록
ord-15ba7c8842c246b2ba780fbfe5aa43cf
출처 데이터셋
uspto-grants-1999_06
특허 번호
US05908615

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