참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-Propanol | HCID 1031 | — |
| 반응물 | Ferulic Acid | HCID 445858 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | n-Propyl ferulate | HCID 9881169 | 64.3% |
반응 단계
In a three-necked flask, 19.4 g (0.1 mole) of ferulic acid, 6.01 g (0.1 mole) of n-propyl alcohol, and 1.0 g of paratoluenesulfonic acid were placed, and 200 ml of benzene was added. This reaction mixture was stirred at 78° C. for 15 hours. Thereafter, the same procedures were taken as in Example 1 to obtain 15.2 g (yield: 64%) of n-propyl ferulate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05908615 |
|---|
| 출처 데이터셋 | uspto-grants-1999_06 |
|---|
| ORD ID | ord-15ba7c8842c246b2ba780fbfe5aa43cf |
|---|
| 출처 메모 | uspto-grants-1999_06 |
|---|
