2-Methoxybenzoyl chloride → HCID 54128447, 화합물

반응식

[C:1]1([C:7]2[C:8]3[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][C:9]=3[S:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:18][O:19][C:20]1[CH:28]=[CH:27][CH:26]=[CH:25][C:21]=1[C:22](Cl)=[O:23]>>[CH3:18][O:19][C:20]1[CH:28]=[CH:27][CH:26]=[CH:25][C:21]=1[C:22]([C:11]1[S:10][C:9]2[CH:12]=[C:13]([O:16][CH3:17])[CH:14]=[CH:15][C:8]=2[C:7]=1[C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)=[O:23]

참가 물질

반응물 2

HCID 889692-Methoxybenzoyl chloride

HCID 15422638HCID 15422638, 화합물

생성물 1

HCID 54128447HCID 54128447, 화합물수율 97%

실험 절차

3-Phenyl-6-methoxybenzo[b]thiophene and 2-methoxybenzoyl chloride were converted to the title compound by the procedure of Example 1 in 97% yield, after crystallization from methanol.

출처 및 근거

ORD 기록: ord-e6f5179fe527472fa2097b11b3fdbcd9
출처 데이터셋: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05908859

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