Sulfanilamide → N-(3-Fluoro-4-methoxybenzylidene)-4-sulfamoylaniline

HRID 1415802

반응식

[F:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[O:10][CH3:11])[CH:5]=O.[S:12]([C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1)(=[O:15])(=[O:14])[NH2:13]>>[F:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[O:10][CH3:11])[CH:5]=[N:20][C:19]1[CH:21]=[CH:22][C:16]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:17][CH:18]=1

참가 물질

반응물 2

HCID 5333Sulfanilamide

HCID 676963-Fluoro-p-anisaldehyde

생성물 1

HCID 21862836N-(3-Fluoro-4-methoxybenzylidene)-4-sulfamoylaniline

실험 절차

Following a procedure similar to that described in Example 1(i), but using 3-fluoro-4-methoxybenzaldehyde and 4-sulfamoylaniline as starting materials, the title compound was obtained as a slightly yellow powder (yield 57%).

출처 및 근거

ORD 기록: ord-210eb2742a674f94b4a83f18f239b058
출처 데이터셋: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05908858

연결된 노트

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