2-(Benzyloxy)-6-bromonaphthalene → HCID 54206028, 화합물

HRID 1416195

반응식

HRID 1416195 반응식
Br[C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([O:12][CH2:13][C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[CH:8]=2)[CH:3]=1.[C:20]([O:24][C:25]([N:27]1[CH2:32][CH2:31][C:30](=[O:33])[CH2:29][CH2:28]1)=[O:26])([CH3:23])([CH3:22])[CH3:21]>>[C:20]([O:24][C:25]([N:27]1[CH2:32][CH2:31][C:30]([OH:33])([C:2]2[CH:11]=[CH:10][C:9]3[C:4](=[CH:5][CH:6]=[C:7]([O:12][CH2:13][C:14]4[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=4)[CH:8]=3)[CH:3]=2)[CH2:29][CH2:28]1)=[O:26])([CH3:23])([CH3:21])[CH3:22]

참가 물질

3

반응물 2

HCID 6405952-(Benzyloxy)-6-bromonaphthaleneHCID 735900tert-Butyl 4-oxopiperidine-1-carboxylate

생성물 1

HCID 54206028HCID 54206028, 화합물수율 33.5%

실험 절차

Beginning with 5.0 gm (15.9 mMol) 2-bromo-6-benzyloxynaphthalene and 3.34 gm (16.8 mMol) 1-tert-butyloxycarbonyl-4-piperidone, 2.31 gm (33%) of the title compound were recovered as a white solid by the procedure described in Preparation I.

출처 및 근거

ORD 기록
ord-7d8ed1570f6a42909c8422ff2fe732ec
출처 데이터셋
uspto-grants-1999_06
특허 번호
US05912256

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