Methanol → Monomethyl maleate

HRID 1416588

반응식

HRID 1416588 반응식
[C:1]1(=[O:7])[O:6][C:4](=[O:5])[CH:3]=[CH:2]1.[CH3:8][OH:9]>>[CH3:8][O:9][C:4](=[O:5])/[CH:3]=[CH:2]\[C:1]([OH:6])=[O:7]

참가 물질

3

반응물 2

HCID 887Methanol2회HCID 7923Maleic Anhydride

생성물 1

HCID 5354456Monomethyl maleate

실험 절차

The same procedure as that of process (I) of Example 1 was conducted to obtain a 50% by weight methanol solution of (A1). In the same manner, to a 1 liter flask were added 24.00 g of maleic anhydride and 39.68 g of methanol, and the resulting mixture was stirred under reflux in a water bath kept at 90° C. Thirty minutes after initiation of the stirring, solid components disappeared, 3 hours after, the temperature was lowered to room temperature to obtain a 50% by weight methanol solution of maleic monomethyl ester.

후처리

  1. temperatureunder reflux in a water bath
  2. customkept at 90° C
  3. customwas lowered to room temperature

출처 및 근거

ORD 기록
ord-cc36d2f1e923404c8fb8aef00087bf94
출처 데이터셋
uspto-grants-1999_06
특허 번호
US05914385

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