Taurine → Magnesium taurate

HRID 1417128노트

반응식

HRID 1417128 반응식
[OH-].[Mg+2:2].[OH-].[NH2:4][CH2:5][CH2:6][S:7]([OH:10])(=[O:9])=[O:8]>O>[CH2:5]([NH2:4])[CH2:6][S:7]([O-:10])(=[O:9])=[O:8].[CH2:5]([NH2:4])[CH2:6][S:7]([O-:10])(=[O:9])=[O:8].[Mg+2:2]

참가 물질

4

반응물 2

HCID 1123TaurineHCID 73981Magnesium Hydroxide

생성물 1

HCID 13343447Magnesium taurate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A mixture of magnesium hydroxide (9.50 g, 8.62 mmol) and taurine (2.16 g, 17.2 mmol) in 20 ml water was refluxed for 7 hours, then evaporated under vacuum to remove most of the water. The paste was diluted with 10 ml ethanol, and after two hours the solid was collected by filtration and dried. Magnesium taurate was obtained as a white powder (about 99% yield). Magnesium taurate could also be obtained as a white powder by lyophilization or by further drying of the paste remaining after evaporation of the reaction mixture.

후처리

  1. temperaturewas refluxed for 7 hours
  2. customevaporated under vacuum
  3. customto remove most of the water
  4. additionThe paste was diluted with 10 ml ethanol
  5. filtrationafter two hours the solid was collected by filtration
  6. customdried

출처 및 근거

ORD 기록
ord-6071a7626a9741e7874a0eab48937e5a
출처 데이터셋
uspto-grants-1999_03
특허 번호
US05876757

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