참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Anthranilic Acid | HCID 227 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | n-Octyl p-Toluenesulfonate | HCID 599296 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-n-octylanthranilic acid | HCID 15090289 | 43.1% |
반응 단계
To a solution of anthranilic acid in toluene, n-octyl p-toluenesulfonate prepared according to the conventional method was added and the mixture was refluxed at 120° C. After 6 hours, an aqueous solution of sodium hydroxide was added and the toluene layer was concentrated. N-n-octylanthranilic acid was obtained from the remaining reactant after the purification by column chromatography with the yield of 43.1%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | USRE036138 |
|---|
| 출처 데이터셋 | uspto-grants-1999_03 |
|---|
| ORD ID | ord-0a2f80ccf9de44bfa5b72d1f02ba953f |
|---|
| 출처 메모 | uspto-grants-1999_03 |
|---|
