1-Piperazinecarboxaldehyde → HCID 86753877, 화합물

HRID 1418344노트

반응식

HRID 1418344 반응식
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S:11]([NH:14][C:15]2[C:20]([O:21][C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=3[O:28][CH3:29])=[C:19]([Cl:30])[N:18]=[C:17](Cl)[N:16]=2)(=[O:13])=[O:12])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[CH:32]([N:34]1[CH2:39][CH2:38][NH:37][CH2:36][CH2:35]1)=[O:33]>>[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S:11]([NH:14][C:15]2[C:20]([O:21][C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=3[O:28][CH3:29])=[C:19]([Cl:30])[N:18]=[C:17]([N:37]3[CH2:38][CH2:39][N:34]([CH:32]=[O:33])[CH2:35][CH2:36]3)[N:16]=2)(=[O:13])=[O:12])=[CH:7][CH:6]=1)([CH3:4])([CH3:2])[CH3:3]

참가 물질

3

반응물 2

HCID 821911-PiperazinecarboxaldehydeHCID 867538724-t-butyl-N-[2,6-dichloro-5-(2-methoxyphenoxy)-4-pyrimidinyl]benzenesulfonamide

생성물 1

HCID 86753877HCID 86753877, 화합물

실험 절차

The procedure described in Synthesis Example 2 was repeated by use of 4-t-butyl-N-[2,6-dichloro-5-(2 -methoxyphenoxy)-4-pyrimidinyl]benzenesulfonamide (5) and 1-formylpiperazine, to thereby obtain the title compound as a pale yellow oil.

후처리

  1. customThe procedure described in Synthesis Example 2

출처 및 근거

ORD 기록
ord-3f2b8757dc0147d8b90feb78703e1bbc
출처 데이터셋
uspto-grants-1999_03
특허 번호
US05883092

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