Ethanol → HCID 70185499, 화합물

HRID 1419180노트

반응식

HRID 1419180 반응식
[C:1]([C:3]1[CH:8]=[CH:7][C:6]([NH:9][C:10](=[O:19])[C:11]([C:17]#[N:18])=[C:12]([CH:14]2[CH2:16][CH2:15]2)[OH:13])=[CH:5][CH:4]=1)#[N:2].C(O)C.O.[NH2:24][C@H:25]([C:31]([OH:33])=[O:32])[CH2:26][CH2:27][CH2:28][CH2:29][NH2:30]>O>[NH2:24][C@H:25]([C:31]([OH:33])=[O:32])[CH2:26][CH2:27][CH2:28][CH2:29][NH2:30].[C:1]([C:3]1[CH:4]=[CH:5][C:6]([NH:9][C:10](=[O:19])[C:11]([C:17]#[N:18])=[C:12]([CH:14]2[CH2:15][CH2:16]2)[OH:13])=[CH:7][CH:8]=1)#[N:2]

참가 물질

5

반응물 3

HCID 702Ethanol2회HCID 16211825Lysine MonohydrateHCID 676596362-Cyano-N-(4-cyanophenyl)-3-cyclopropyl-3-hydroxyprop-2-enamide

생성물 1

HCID 70185499HCID 70185499, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

15 g (0.054 mol) of 2-cyano-3-cyclopropyl-3-hydroxyacrylic acid (4-cyanophenyl)amide are dissolved in 900 ml of water and 10 ml of ethanol together with 9.6 g (0.054 mol) of L-lysine hydrate, filtered and lyophilized. Adhering residual amounts of ethanol are removed by drying under reduced pressure.

후처리

  1. customare removed
  2. customby drying under reduced pressure

출처 및 근거

ORD 기록
ord-b860c63b5bf6476286efbc51b879a201
출처 데이터셋
uspto-grants-1999_03
특허 번호
US05886033

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