Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chlorobiphenyl → 2-(2-Iodophenyl)ethan-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chlorobiphenyl | HCID 16323 | — |
| 반응물 | 1-(2-Bromoethyl)-2-iodobenzene | HCID 11077801 | — |
| 반응물 | Phenylpropyl malonate | HCID 86753570 | — |
| 생성물 | 2-(2-Iodophenyl)ethan-1-ol | HCID 11064750 | — |
반응 단계
The title compound was synthesized by a sequence similar to that for Example 87 except that 2-(2-iodophenyl)ethyl bromide and commercially available diethyl phenethyl malonate were used in lieu of the 4-chlorobiphenyl and phenylpropyl malonate respectively. The final product was recrystallized from chloroform to give a fluffy, white solid (mp: melts/softens over a broad range starting at 50° C.; the bulk of the sample melts at 189°-190° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05886024 |
| 출처 데이터셋 | uspto-grants-1999_03 |
| ORD ID | ord-85fe9cb35a9243cfaf8edd9d1c8b6108 |
| 출처 메모 | uspto-grants-1999_03 |