Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
9,10-Difluoro-2-bromo-7-octylphenanthrene → 9,10-Difluoro-2-hexyl-7-octylphenanthrene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 9,10-Difluoro-2-bromo-7-octylphenanthrene | HCID 54084199 | — |
| 반응물 | HCID 178444609 | HCID 178444609 | — |
| 생성물 | 9,10-Difluoro-2-hexyl-7-octylphenanthrene | HCID 53665512 | — |
반응 단계
In analogy to Example 2, from 9,10-difluoro-2-bromo-7-octylphenanthrene and 10 mmol of hexylmagnesium bromide. The catalyst used is 0.2 mmol of 1,3-bis(diphenylphosphine)propanenickel(lI) chloride. Chromatography gives 9,10-difluoro-2-hexyl-7-octylphenanthrene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05888422 |
| 출처 데이터셋 | uspto-grants-1999_03 |
| ORD ID | ord-c2632c3f02294a9f8820667c0bf2c9c5 |
| 출처 메모 | uspto-grants-1999_03 |