반응식
Cl.[NH2:2][C:3]1[CH:7]=[C:6]([Cl:8])[S:5][C:4]=1[S:9]([NH2:12])(=[O:11])=[O:10].[CH3:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][N:19]=[C:20]=S>>[Cl:8][C:6]1[S:5][C:4]2[S:9](=[O:10])(=[O:11])[N:12]=[C:20]([NH:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH3:13])[NH:2][C:3]=2[CH:7]=1참가 물질
3
실험 절차
The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and n-hexyl isothiocyanate by a procedure analogous to the procedure described in example 3Bc-d; mp 207°-209° C.; 1H-NMR (DMSO-d6): δ 0.87 (distorted t, 3H), 1.28 (m, 6H), 1.51 (m, 2H), 3.17 (q, 2H), 7.05 (s, 1H), 7.30 (br. s, 1H), 11.01 (s, 1H).
출처 및 근거
- ORD 기록
- ord-9f9a7ea5c10a4aac9469a3c0cbd497e7
- 출처 데이터셋
- uspto-grants-1999_03
- 특허 번호
- US05889002
연결된 노트
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