Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide → HCID 178418472, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide | HCID 53745902 | — |
| 반응물 | Sodium hydrogen sulphide | HCID 86586439 | — |
| 생성물 | HCID 178418472 | HCID 178418472 | 63.6% |
반응 단계
Using the procedure in Preparation 34, 6.4 g (0.02 mol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide was reacted with 4.8 g (0.066 mol) of sodium hydrogen sulfide to afford 4.2 g of the title compound, mp 178°-180° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05889034 |
| 출처 데이터셋 | uspto-grants-1999_03 |
| ORD ID | ord-bd7d005154984883b5bd36cf3a93424c |
| 출처 메모 | uspto-grants-1999_03 |