Water → HCID 18781954, 화합물
반응식
Br[CH2:2][CH2:3][CH2:4][C:5]([O:7][CH2:8][CH:9]=[CH2:10])=[O:6].[C:11]([O-:14])(=[S:13])[CH3:12].[K+].O>CN(C)C=O>[C:11]([S:13][CH2:2][CH2:3][CH2:4][C:5]([O:7][CH2:8][CH:9]=[CH2:10])=[O:6])(=[O:14])[CH3:12]참가 물질
5
실험 절차
Allyl 4-bromobutyrate (19.7 g) was treated with potassium thioacetate (10.9 g) in dimethyl formamide (100 ml) at 20° C. for 2 hours. Water (500 ml) was added and the mixture extracted with diethyl ether. The ethereal solution was washed with dilute aq. HCl, brine, dried (MgSO4) and evaporated to give the title compound as an oil (18.6 g, 97%)
후처리
- extractionthe mixture extracted with diethyl ether
- washThe ethereal solution was washed with dilute aq. HCl, brine
- dry with materialdried (MgSO4)
- customevaporated
출처 및 근거
- ORD 기록
- ord-b9291264b8d44e3c9fbe8b8d145161ba
- 출처 데이터셋
- uspto-grants-2000_06
- 특허 번호
- US06071899
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