참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methane | HCID 297 | — |
| 반응물 | Hexanoic Acid | HCID 8892 | — |
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 생성물 | 3-Aminohexanoic acid | HCID 5275645 | — |
반응 단계
A mixture of 2 hexanoic acid (7.0 g, 0.06 mole) and concentrated aqueous ammonium hydroxide (70 ml) is heated for 24 hours in an autoclave at 150° C. The cooled mixture is treated with carbon black and filtered. After evaporation of the solvent, the crude product is recrystallized from ethanol to give the title compound m.p. 203° C. (Compound 1.21, Table 1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06075051 |
|---|
| 출처 데이터셋 | uspto-grants-2000_06 |
|---|
| ORD ID | ord-3e066ec21d4e4a9d8864e13b0a802682 |
|---|
| 출처 메모 | uspto-grants-2000_06 |
|---|
