Triethylamine → Methyl 3-[2-[2-(4-fluorophenyl)ethoxy]ethylaminosulphonyl]propanoate
반응식
[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][O:10][CH2:11][CH2:12][NH2:13])=[CH:4][CH:3]=1.C(N(CC)CC)C.Cl[S:22]([CH2:25][CH2:26][C:27]([O:29][CH3:30])=[O:28])(=[O:24])=[O:23]>C(OCC)C>[F:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][CH2:9][O:10][CH2:11][CH2:12][NH:13][S:22]([CH2:25][CH2:26][C:27]([O:29][CH3:30])=[O:28])(=[O:24])=[O:23])=[CH:6][CH:7]=1참가 물질
5
실험 절차
The subtitle compound (8.32 g) was prepared according to the method of Example 3d) using 2-[2-(4-fluorophenyl)ethoxy]ethanamine (5.36 g), triethylamine (4.6 ml) and methyl 3-(chlorosulphonyl)propanoate (5.6 g) in diethyl ether (150 ml).
출처 및 근거
- ORD 기록
- ord-6019977ba8484c869a7bf7ef54b84628
- 출처 데이터셋
- uspto-grants-2000_06
- 특허 번호
- US06080869
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