Pyridine → 1-Butylpyridinium bromide
반응식
[Br:1][CH2:2][CH2:3][CH2:4][CH3:5].[N:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>>[Br-:1].[CH2:2]([N+:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[CH2:3][CH2:4][CH3:5]참가 물질
3
실험 절차
Butylpyridinium bromide is prepared by a Menshutkin reaction of 27.5 g of 1-bromobutane with 15.8 g of pyridine at 40° C. in 24 hours, without solvent. The solid obtained is dried under low vacuum at 50° C.
후처리
- customThe solid obtained
- customis dried under low vacuum at 50° C.
출처 및 근거
- ORD 기록
- ord-f6f3807a53504064978aa6558408ba26
- 출처 데이터셋
- uspto-grants-2015_01
- 특허 번호
- US08927160B2
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