4-(Propan-2-yl)benzene-1,2-diamine → HCID 178496737, 화합물

반응식

[CH3:1][CH:2]([C:4]1[CH:5]=[C:6]([NH2:11])[C:7]([NH2:10])=[CH:8][CH:9]=1)[CH3:3].C(OC([NH:19][C@H:20]([C:25](O)=O)[C@@H:21]([CH3:24])[O:22][CH3:23])=O)(C)(C)C>>[CH3:23][O:22][C@H:21]([CH3:24])[C@@H:20]([C:25]1[NH:10][C:7]2[CH:8]=[CH:9][C:4]([CH:2]([CH3:1])[CH3:3])=[CH:5][C:6]=2[N:11]=1)[NH2:19]

참가 물질

반응물 2

HCID 50970284-(Propan-2-yl)benzene-1,2-diamine

HCID 15460346(2S,3R)-2-{[(tert-butoxy)carbonyl]amino}-3-methoxybutanoic acid

생성물 1

HCID 178496737HCID 178496737, 화합물

실험 절차

The title compound was prepared according to Method 4 using 4-(1-methylethyl)-1,2-benzenediamine and N-(tert-butoxycarbonyl)-O-methyl-L-threonine (Preparation 51). The residue was purified by elution through an SCX cartridge.

후처리

customThe residue was purified by elution through an SCX cartridge

출처 및 근거

ORD 기록: ord-a435b4d5079b4c42ba7165f27a0ec0cd
출처 데이터셋: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08927587B2

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