Chlorosuccinimide → HCID 67548928, 화합물

반응식

[CH3:1][C:2]1[NH:6][C:5]([C:7]([O:9][CH2:10][CH3:11])=[O:8])=[N:4][CH:3]=1.C1C(=O)N([Cl:19])C(=O)C1>>[Cl:19][C:3]1[N:4]=[C:5]([C:7]([O:9][CH2:10][CH3:11])=[O:8])[NH:6][C:2]=1[CH3:1]

참가 물질

반응물 2

HCID 31398Chlorosuccinimide

HCID 24974466Ethyl 5-methyl-1H-imidazole-2-carboxylate

생성물 1

HCID 67548928HCID 67548928, 화합물수율 82.1%

실험 절차

The same operation as in Example (1c) was performed using ethyl 5-methyl-1H-imidazole-2-carboxylate obtained in Example (5a) (0.50 g, 3.23 mmol) and NCS (0.44 g, 3.25 mmol), to obtain 0.50 g of the title compound as a white solid (82%).

출처 및 근거

ORD 기록: ord-ba1da1aa692f45ee90161a371a08174b
출처 데이터셋: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08927588B2

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