1-Bromo-3-methylbutan-2-one → 2-(3-Methyl-2-oxobutyl)-1h-isoindole-1,3(2h)-dione
반응식
Br[CH2:2][C:3](=[O:7])[CH:4]([CH3:6])[CH3:5].[C:8]1(=[O:18])[NH:12][C:11](=[O:13])[C:10]2=[CH:14][CH:15]=[CH:16][CH:17]=[C:9]12.[K]>>[CH3:5][CH:4]([CH3:6])[C:3](=[O:7])[CH2:2][N:12]1[C:8](=[O:18])[C:9]2[C:10](=[CH:14][CH:15]=[CH:16][CH:17]=2)[C:11]1=[O:13]참가 물질
3
실험 절차
The same operation as in Example (15b) was performed using 1-bromo-3-methylbutan-2-one obtained in Example (35a) (3.94 g, 23.9 mmol) and potassium phthalimide (4.4 g, 23.8 mmol), to obtain 4.08 g of the title compound as a white solid (74%).
출처 및 근거
- ORD 기록
- ord-6a293d2b6a3c49d798a810cf1f8b1e2c
- 출처 데이터셋
- uspto-grants-2015_01
- 특허 번호
- US08927588B2
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