반응식
C[O:2][CH:3](OC)[C:4]1[NH:5][C:6]([CH3:13])=[C:7]([C:9]([F:12])([F:11])[F:10])[N:8]=1.S(=O)(=O)(O)O>>[CH3:13][C:6]1[NH:5][C:4]([CH:3]=[O:2])=[N:8][C:7]=1[C:9]([F:12])([F:10])[F:11]참가 물질
3
실험 절차
The same operation as in Example (33b) was performed using 2-(dimethoxymethyl)-5-methyl-4-(trifluoromethyl)-1H-imidazole obtained in Example (36b) (about 2.17 mmol) and 2 N sulfuric acid (15 mL), to obtain 30.5 mg of the title compound as a white solid (7.9%).
출처 및 근거
- ORD 기록
- ord-c55dfe9fca174aa999afdb02641b211a
- 출처 데이터셋
- uspto-grants-2015_01
- 특허 번호
- US08927588B2
연결된 노트
불러오는 중…