1,4-Butane sultone → Sodium 2,3,3-Trimethyl-1-(3-sulfonatobutyl)-3H-indolium-5-sulfonate

반응식

[CH3:1][C:2]1[C:10]([CH3:12])([CH3:11])[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([S:13]([O-:16])(=[O:15])=[O:14])[CH:8]=2)[N+:3]=1[CH2:17][CH2:18][CH2:19][S:20]([O-:23])(=[O:22])=[O:21].[Na+:24].[CH2:25]1COS(=O)(=O)CC1>>[CH3:1][C:2]1[C:10]([CH3:11])([CH3:12])[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([S:13]([O-:16])(=[O:15])=[O:14])[CH:8]=2)[N+:3]=1[CH2:17][CH2:18][CH:19]([S:20]([O-:23])(=[O:22])=[O:21])[CH3:25].[Na+:24]

참가 물질

반응물 2

HCID 154111,4-Butane sultone

HCID 71692790Sodium 2,3,3-Trimethyl-1-(3-sulfonatopropyl)-3H-indolium-5-sulfonate

생성물 1

HCID 87428036Sodium 2,3,3-Trimethyl-1-(3-sulfonatobutyl)-3H-indolium-5-sulfonate

실험 절차

Compound 38 is prepared analogously to compound 4 (Example 4), except that 1,4-butanesultone is used as a starting material.

출처 및 근거

ORD 기록: ord-8bd252ec720549bfa20efdaddc361ca5
출처 데이터셋: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08927719B2

반응 노트

불러오는 중…