HCID 71059611, 화합물 → HCID 86674220, 화합물

HRID 1425599노트

반응식

HRID 1425599 반응식
C([O:8][C:9]1[CH:21]=[N:20][C:19]2[C:18]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=3[NH:12][C:11]=2[CH:10]=1)C1C=CC=CC=1>CO.[Pd]>[N:20]1[C:19]2[C:18]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=3[NH:12][C:11]=2[CH:10]=[C:9]([OH:8])[CH:21]=1

참가 물질

4

반응물 1

HCID 71059611HCID 71059611, 화합물

생성물 1

HCID 86674220HCID 86674220, 화합물수율 99.4%

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

3-(benzyloxy)-5H-pyrido[3,2-b]indole (0.09 g, 0.328 mmol) and Palladium 10% on carbon (0.035 g, 0.033 mmol) in MeOH (Volume: 5 ml) was stirred under hydrogen for 2 hours. Filtered and concentrated to afford 5H-pyrido[3,2-b]indol-3-ol (0.06 g, 0.326 mmol, 99% yield).

후처리

  1. filtrationFiltered
  2. concentrationconcentrated

출처 및 근거

ORD 기록
ord-bcad21fa92484fe6ba03e4fdb2f40598
출처 데이터셋
uspto-grants-2015_01
특허 번호
US08932557B2

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