Phenylacetylene → HCID 53247204, 화합물

반응식

Br[C:2]1[CH:3]=[N:4][C:5]2[N:6]([N:8]=[C:9]([CH:11]3[CH2:14][CH2:13][CH2:12]3)[CH:10]=2)[CH:7]=1.[C:15]1([C:21]#[CH:22])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH:11]1([C:9]2[CH:10]=[C:5]3[N:4]=[CH:3][C:2]([C:22]#[C:21][C:15]4[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=4)=[CH:7][N:6]3[N:8]=2)[CH2:14][CH2:13][CH2:12]1

참가 물질

반응물 2

HCID 10821Phenylacetylene

HCID 58316713HCID 58316713, 화합물

생성물 1

HCID 53247204HCID 53247204, 화합물

실험 절차

The title compound, light brown solid, MS: m/e=274.3 (M+H+), can be prepared in accordance with the general method of example 1 from 6-bromo-2-cyclobutyl-pyrazolo[1,5-a]pyrimidine (example 18, step 1) and phenylacetylene.

출처 및 근거

ORD 기록: ord-68ae431de3344a9bb14908273843c046
출처 데이터셋: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08933094B2

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