Phenylacetylene → HCID 53247568, 화합물

반응식

[C:1]([C:5]1[N:14]=[C:8]2[CH:9]=[CH:10][C:11](I)=[CH:12][N:7]2[N:6]=1)([CH3:4])([CH3:3])[CH3:2].[C:15]1([C:21]#[CH:22])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[C:1]([C:5]1[N:14]=[C:8]2[CH:9]=[CH:10][C:11]([C:22]#[C:21][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)=[CH:12][N:7]2[N:6]=1)([CH3:4])([CH3:3])[CH3:2]

참가 물질

반응물 2

HCID 10821Phenylacetylene

HCID 58316712HCID 58316712, 화합물

생성물 1

HCID 53247568HCID 53247568, 화합물

실험 절차

The title compound, a yellow solid, MS: m/e=276.2 (M+H+), can be prepared in accordance with the general method of example 1 from 2-tert-butyl-6-iodo-[1,2,4]triazolo[1,5-a]pyridine (example 39, step 4) and phenylacetylene.

출처 및 근거

ORD 기록: ord-32c693ea51264e818096677aa82d614f
출처 데이터셋: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08933094B2

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